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The Art of Carbohydrate AnalysisAnalysis of Carbohydrates by Nuclear Magnetic Resonance SpectroscopyNuclear magnetic resonance spectroscopy (NMR)

The Art of Carbohydrate Analysis: Analysis of Carbohydrates by Nuclear Magnetic Resonance... [NMR spectroscopy has shown to be extremely useful for the characterization of glycan structures. Carbohydrates have two natural NMR-active nuclei: 1H and 13C. This chapter describes the identification of monosaccharides and glycans by the assignment of their protons and carbons, using the structural-reporter group concept and 2D NMR techniques, which additionally provide linkage and sequence information. All this is illustrated by some NMR spectra of glycans and polysaccharides and the NMR measuring procedure is summarized.] http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png

The Art of Carbohydrate AnalysisAnalysis of Carbohydrates by Nuclear Magnetic Resonance SpectroscopyNuclear magnetic resonance spectroscopy (NMR)

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References (20)

Publisher
Springer International Publishing
Copyright
© Springer Nature Switzerland AG 2021
ISBN
978-3-030-77790-6
Pages
273 –296
DOI
10.1007/978-3-030-77791-3_12
Publisher site
See Chapter on Publisher Site

Abstract

[NMR spectroscopy has shown to be extremely useful for the characterization of glycan structures. Carbohydrates have two natural NMR-active nuclei: 1H and 13C. This chapter describes the identification of monosaccharides and glycans by the assignment of their protons and carbons, using the structural-reporter group concept and 2D NMR techniques, which additionally provide linkage and sequence information. All this is illustrated by some NMR spectra of glycans and polysaccharides and the NMR measuring procedure is summarized.]

Published: Oct 24, 2021

Keywords: Cryoprobe; Fourier transformation; CASPER; Free induction decay; Chemical shift; Vicinal coupling constant; Deuterium; Bulk region; COSY; TOCSY; HMBC; NOESY; ROESY; HSQC; MAS-NMR; N-glycan; Polysaccharide; α-glucan

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