Access the full text.
Sign up today, get DeepDyve free for 14 days.
Loading next page...
/lp/springer-journals/the-art-of-carbohydrate-analysis-monosaccharide-composition-analysis-3a0LAjEyIj
References (22)
-
Chun-Hung Lin, Chien-Yuan Kuo, Kuo-Shiang Liao, Wen-bin Yang (2011)
Monosaccharide-NAIM Derivatives for D-, L-Configurational AnalysisMolecules, 16
-
G. Gerwig, H. Hocking, R. Stöcklin, J. Kamerling, R. Boelens (2013)
Glycosylation of ConotoxinsMarine Drugs, 11
-
Gerit Gerwig, J. Kamerling, J. Vliegenthart (1979)
Determination of the absolute configuration of mono-saccharides in complex carbohydrates by capillary G.L.C.Carbohydrate research, 77
-
Yan-Hong Wang, B. Avula, Xiang Fu, Mei Wang, I. Khan (2012)
Simultaneous Determination of the Absolute Configuration of Twelve Monosaccharide Enantiomers from Natural Products in a Single Injection by a UPLC-UV/MS MethodPlanta Medica, 78
-
W. Morelle, J. Michalski (2007)
Analysis of protein glycosylation by mass spectrometryNature Protocols, 2
-
I. Pasha, F. Ahmad (2021)
Monosaccharide composition and carbohydrates linkage identification in cereal brans using UHPLC/QqQ-DMRM-MSJournal of Food Composition and Analysis, 96
-
G. Sassaki, L. Souza (2013)
Mass Spectrometry Strategies for Structural Analysis of Carbohydrates and Glycoconjugates -
N. Price (2008)
Permethylation Linkage Analysis Techniques for Residual CarbohydratesApplied Biochemistry and Biotechnology, 148
-
Jun Han, Karen Lin, Carita Sequria, Juncong Yang, C. Borchers (2016)
Quantitation of low molecular weight sugars by chemical derivatization‐liquid chromatography/multiple reaction monitoring/mass spectrometryELECTROPHORESIS, 37
-
Ace Galermo, E. Nandita, Mariana Barboza, Matthew Amicucci, Thai Vo, C. Lebrilla (2018)
Liquid Chromatography-Tandem Mass Spectrometry Approach for Determining Glycosidic Linkages.Analytical chemistry, 90 21
-
K. Mariño, J. Bones, J. Kattla, P. Rudd (2010)
A systematic approach to protein glycosylation analysis: a path through the maze.Nature chemical biology, 6 10
-
L. Ruhaak, C. Lebrilla (2015)
Applications of Multiple Reaction Monitoring to Clinical GlycomicsChromatographia, 78
-
G. Cooper, Minakshi Sant, Cynthia Asiyo (2009)
Gas chromatography-mass spectrometry resolution of sugar acid enantiomers on a permethylated beta-cyclodextrin stationary phase.Journal of chromatography. A, 1216 40
-
I. Ciucanu (2006)
Per-O-methylation reaction for structural analysis of carbohydrates by mass spectrometry.Analytica chimica acta, 576 2
-
Takashi Tanaka, Tatsuya Nakashima, T. Ueda, K. Tomii, I. Kouno (2007)
Facile discrimination of aldose enantiomers by reversed-phase HPLC.Chemical & pharmaceutical bulletin, 55 6
-
W. König, I. Benecke, H. Bretting (1981)
Gas Chromatographic Separation of Carbohydrate Enantiomers on a New Chiral Stationary PhaseAngewandte Chemie, 20
-
Zhenqing Zhang, N. Khan, K. Nuñez, E. Chess, C. Szabo (2012)
Complete monosaccharide analysis by high-performance anion-exchange chromatography with pulsed amperometric detection.Analytical chemistry, 84 9
-
Gege Xu, Matthew Amicucci, Zhi Cheng, Ace Galermo, C. Lebrilla (2018)
Revisiting monosaccharide analysis - quantitation of a comprehensive set of monosaccharides using dynamic multiple reaction monitoring.The Analyst, 143 1
-
S. Kodama, S. Aizawa, A. Taga, Tomohisa Yamashita, Tomoko Kemmei, A. Yamamoto, K. Hayakawa (2007)
Simultaneous chiral resolution of monosaccharides as 8‐aminonaphthalene‐1,3,6‐trisulfonate derivatives by ligand‐exchange CE using borate as a central ion of the chiral selectorELECTROPHORESIS, 28
-
G. Gerwig, J. Kamerling, J. Vliegenthart (1978)
Determination of the d and l configuration of neutral monosaccharides by high-resolution capillary g.l.c.Carbohydrate Research, 62
-
I. Sims, Susan Carnachan, T. Bell, S. Hinkley (2018)
Methylation analysis of polysaccharides: Technical advice.Carbohydrate polymers, 188
-
João Lopes, E. Gaspar (2008)
Simultaneous chromatographic separation of enantiomers, anomers and structural isomers of some biologically relevant monosaccharides.Journal of chromatography. A, 1188 1
- Publisher
- Springer International Publishing
- Copyright
- © Springer Nature Switzerland AG 2021
- ISBN
- 978-3-030-77790-6
- Pages
- 127 –156
- DOI
- 10.1007/978-3-030-77791-3_6
- Publisher site
- See Chapter on Publisher Site
Abstract
[A monosaccharide composition determination is the first step in the process of characterizing complex carbohydrate. Two frequently used methods, gas chromatography and high-performance liquid chromatography, will be discussed. Usually, the second step in carbohydrate structure characterization is the determination of the linkage types of the constituting monosaccharides. These assignments are obtained by gas–liquid chromatography-mass spectrometry. This chapter provides detailed protocols for monosaccharide and linkage analysis, as well as the absolute configuration (d/l) determination.]
Published: Oct 24, 2021
Keywords: HPLC; HPAEC; GC-MS; CE; TLC; EI-MS; Hydrolysis; Methanolysis; Trimethylsilylation; TMS methyl glycosides; Permethylation; Alditol acetates; PMAA