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The unique phase in a crystal of triphenylsilanol (Ph3SiOH) is reported. It is observed that after the crystal is flash‐cooled from room temperature to 100 K, a new stable ordered phase II occurs with an increase in the unit‐cell parameters compared to the earlier reported phase I. The new phase II occurs upon fast cooling while on slow cooling the disordered phase I is present. Gradual heating from 100 K (phase II) causes the crystal to return to the original phase I at about 150 K. The crystal undergoes the observed transformation in a reversible manner in many consecutive flash cooling/heating cycles without cracking.
Acta Crystallographica Section B – Wiley
Published: Jun 1, 2023
Keywords: triphenylsilanol; flash cooling; crystal structure
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